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Edoxaban(依度沙班)
480449-70-5;912273-65-5
N-(5-chloropyridin-2-yl)-N'-[(1S,2R,4S)-4-(N,N-dimethylcarbamoyl)-2-(5-methyl-4,5,6,7-tetrahydro[1,3]thiazolo[5,4-c]pyridine-2-carboxamido)cyclohexyl]oxamide
C24H30ClN7O4S
548.06
Pale Yellow Powder
≥98% by HPLC
HPLC,H-NMR,13C-NMR,MS
Edoxaban Impurity A
tert-butyl ((1R,2S,5S)-2-(2-((5-chloropyridin-2-yl)amino)-2-oxoacetamido)-5-(dimethylcarbamoyl)cyclohexyl)carbamate
C21H30ClN5O5
467.95
Pale Yellow Powder
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity B
N1-((1S,2R,4S)-2-amino-4-(dimethylcarbamoyl)cyclohexyl)-N2-(5-chloropyridin-2-yl)oxalamide
C16H22ClN5O3
367.83
Off-White to Pale Yellow Powder
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity C
N1,N1'-((1S,2R,4S)-4-(dimethylcarbamoyl)cyclohexane-1,2-diyl)bis(N2-(5-chloropyridin-2-yl)oxalamide)
C23H25Cl2N7O5
550.39
Off-White to Pale Yellow Powder
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity D
N1-(5-chloropyridin-2-yl)-N2-((1R,2S,5S)-5-(dimethylcarbamoyl)-2-(5-methyl-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamido)cyclohexyl)oxalamide
C24H30ClN7O4S
548.06
Off-White to Pale Yellow Powder
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity E
N,N'-((1S,2R,4S)-4-(dimethylcarbamoyl)cyclohexane-1,2-diyl)bis(5-methyl-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamide)
C25H35N7O3S2
545.72
Off-White to Pale Yellow Powder
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity F
N-((1R,2S,5S)-2-amino-5-(dimethylcarbamoyl)cyclohexyl)-5-methyl-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamide
C17H27N5O2S
365.49
Pale Yellow Powder
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity G
2-(((1S,2R,4S)-4-(dimethylcarbamoyl)-2-(5-methyl-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamido)cyclohexyl)amino)-2-oxoacetic acid
C19H27N5O5S
437.51
Pale Yellow Powder
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity H
2-(((1R,2S,5S)-2-(2-((5-chloropyridin-2-yl)amino)-2-oxoacetamido)-5-(dimethylcarbamoyl)cyclohexyl)carbamoyl)-5-methyl-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine 5-oxide
C24H30ClN7O5S
564.06
Off-White to Pale Yellow Powder
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity I
5-chloro-2-(2-(((1S,2R,4S)-4-(dimethylcarbamoyl)-2-(5-methyl-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamido)cyclohexyl)amino)-2-oxoacetamido)pyridine 1-oxide
C24H30ClN7O5S
564.06
Off-White to Pale Yellow Powder
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity J
(1S,3R,4S)-4-(2-((5-chloropyridin-2-yl)amino)-2-oxoacetamido)-3-(5-methyl-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamido)cyclohexanecarboxylic acid
C22H25ClN6O5S
520.99
Pale Yellow Powder
≥90% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity K
2-(((1R,2S,5S)-2-(2-((5-chloro-1-oxidopyridin-2-yl)amino)-2-oxoacetamido)-5-(dimethylcarbamoyl)cyclohexyl)carbamoyl)-5-methyl-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine 5-oxide
C24H30ClN7O6S
580.06
Off-White to Pale Yellow Powder
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity L
N1-(3,5-dichloropyridin-2-yl)-N2-((1S,2R,4S)-4-(dimethylcarbamoyl)-2-(5-methyl-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamido)cyclohexyl)oxalamide
C24H29Cl2N7O4S
582.50
Off-White to Pale Yellow Powder
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity M
1072-98-6
5-chloropyridin-2-amine
C5H5ClN2
128.56
Off-White Solid
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity N
N1-(5-chloropyridin-2-yl)-N2-(5-methylpyridin-2-yl)oxalamide
C13H11ClN4O2
290.71
Off-White Solid
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity O
552850-73-4
2-((5-chloropyridin-2-yl)amino)-2-oxoacetic acid
C7H5ClN2O3
200.58
Off-White Solid
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity P
ethyl 2-((3,5-dichloropyridin-2-yl)amino)-2-oxoacetate
C9H8Cl2N2O3
263.08
Off-White Solid
≥95% by HPLC
HPLC,H-NMR,MS
Edoxaban Impurity Q
ethyl 2-oxo-2-(pyridin-2-ylamino)acetate
C9H10N2O3
194.19
Off-White Solid
≥95% by HPLC
HPLC,H-NMR,MS
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