HH-BLQ 玻璃球测定药典二氧化碳

玻璃球测定药典二氧化碳

玻璃球测定药典二氧化碳 详细信息：

填充柱：

玻璃球，80目，0.8*4mm，1m*1/8

净化装置

甲烷/N2标准气体

GC-7990气相色谱仪

FID检测器

氮氢空发生器

减压阀

提供完整的分析方案



   碳氢化合物
取本品作为供试品气体，取甲烷含量为0.0020%的气体(以氮气为稀释剂)作为对照气体，照气相色谱法(通则0521)试验，用玻璃球为填料的色谱柱(4mm×0.8m，80目)；柱温为110℃；进样口温度为110℃；检测器为火焰离子化检测器，温度为120℃。量取供试品气体与对照气体，注入色谱仪，在净化温度为360℃时测得的峰面积为相应空白值；量取供试品气体与对照气体，注入色谱仪，测定峰面积，减去相应空白值后的峰面积为校正峰面积。按外标法以校正峰面积计算，含碳氢化合物(以甲烷计)不得过0.0020%。



玻璃球测定药典二氧化碳 测试谱图：







Glass ball determination of pharmacopoeia carbon dioxide

Glass ball determination of pharmacopoeia carbon dioxide Details:

Packed column:

Glass ball, 80 mesh, 0.8*4mm, 1m*1/8

Purification device

Methane/N2 standard gas

GC-7990 Gas Chromatograph

FID detector

Nitrogen hydrogen generator

Pressure reducing valve

Provide a complete analysis solution



    Hydrocarbon is taken as the test gas, and a gas with a methane content of 0.0020% (with nitrogen as a diluent) is used as a control gas, and gas chromatography (General Rule 0521) is used to test the column with glass spheres as a filler ( 4mm × 0.8m, 80 mesh); column temperature is 110 ° C; inlet temperature is 110 ° C; detector is flame ionization detector, temperature is 120 ° C. The test gas and the control gas are measured and injected into the chromatograph. The peak area measured at the purification temperature of 360 ° C is the corresponding blank value; the gas for the test sample and the control gas are taken, injected into the chromatograph, and the peak area is measured and reduced. The peak area after the corresponding blank value is the corrected peak area. According to the external standard method, the hydrocarbon content (in terms of methane) should not exceed 0.0020%.



Glass ball determination of pharmacopoeia carbon dioxide test spectrum: